Hiroshima University Syllabus

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Japanese
Academic Year 2024Year School/Graduate School School of Engineering
Lecture Code K7113030 Subject Classification Specialized Education
Subject Name 化学実験I
Subject Name
(Katakana)
カガクジツケン 1
Subject Name in
English
Chemical Experiments I
Instructor NAKAYAMA YUUSHOU,KAWASAKI RIKU,ADACHI YOHHEI,MIKIE TSUBASA
Instructor
(Katakana)
ナカヤマ ユウショウ,カワサキ リク,アダチ ヨウヘイ,ミキエ ツバサ
Campus Higashi-Hiroshima Semester/Term 3rd-Year,  First Semester,  First Semester
Days, Periods, and Classrooms (1st) Mon5-8,Thur5-8,Fri5-8:ENG B4-008
Lesson Style Experiment Lesson Style
(More Details)
 
Chemical Reagents, Glasswares 
Credits 4.0 Class Hours/Week   Language of Instruction J : Japanese
Course Level 3 : Undergraduate High-Intermediate
Course Area(Area) 25 : Science and Technology
Course Area(Discipline) 07 : Chemistry
Eligible Students Cluster 3, Applied Chemistry
Keywords  
Special Subject for Teacher Education   Special Subject  
Class Status
within Educational
Program
(Applicable only to targeted subjects for undergraduate students)
 
Criterion referenced
Evaluation
(Applicable only to targeted subjects for undergraduate students)
Program of Applied Chemistry
(Knowledge and Understanding)
・Wide range of basic knowledge on liberal arts and specialized education, and professional basic knowledge on chemistry.
・Advanced technical knowledge of applied chemistry.
・The conception ability based on logical thinking supported by basic and technical knowledge.
(Abilities and Skills)
・Creativity to solve various problems related to applied chemistry utilizing acquired knowledge and skills
・Socially acceptable sense of moral and designing ability of research and development, which allow demonstrating the ability to solve issues as a researcher ・engineer.
(Comprehensive Abilities)
・Self-motivating and continuous learning ability
・Attitudes actively trying to take multiple approaches for solving problems as an independent researcher or engineer utilizing the following items: information collection, skill improvement, development of research methods, analysis and understanding of research outcomes and results.
・Abilities for logical description, presentation, and discussion in Japanese language. 
Class Objectives
/Class Outline
Students will learn the following contents through the chemical experiments of several organic reactions:
・Building experiment plans
・Handle of the reaction reagents and solvents
・Handle of labwares
・Reaction operations
・Purification of materials (distillation, recrystallization, extraction, reprecipitation, etc.)
・How to write experiment notebook, report
・Various analyses (GC, LC, TLC, IR, NMR, the molecular weight measurement) 
Class Schedule lesson1: Guidance
lesson2: Theme I Guidance (Installation of ChemDraw, User registration for SciFinder)
lesson3: ChemDraw workshop
lesson4: SciFinder workshop
lesson5: How to write a report
lesson6: How to use a rotary evaporator
lesson7: Separation of neutral, acidic, and basic compounds
lesson8: How to use a chromatography
lesson9: Clean up
lesson10: How to set up a thin layer chromatography (TLC) analysis
lesson11: How to set up a silica-gel chromatography
lesson12: Finishing, Clean up
lesson13: Theme II Guidance
lesson14: Extraction of caffeine from tea
lesson15-17: Extraction of pigments from plants and their purification using silicagel column chromatography
lesson18: Finishing, Clean up
lesson19-20: Preparation of thermo-responsive hydrogel comprising PNIPAM
lesson21-22: Synthesis and characterization of methylorange
lesson23: Finishing, Clean up
lesson24: Theme III Guidance
lesson25: Wittig-Horner reaction
lesson26: E2 reaction
lesson27: Diels-Alder reaction-1
lesson28: Diels-Alder reaction-2
lesson29: Finishing, Clean up
lesson30: Aldol reaction
lesson31: Cross-coupling reaction
lesson32: Synthesis of poly(vinyl acetate)
lesson33: Measurement of Molecular Weight
lesson34: Finishing, Clean up
lesson35: Theme IV guidance
lesson36-37: Synthesis of ferrocene
lesson38: Synthesis of acetylferrocene
lesson39: TLC Analysis of acetylferrocene, Synthesis of 1-hydroxyethylferrocene
lesson40: Synthesis of vinylferrocene
lesson41-42: Copolymerization of MMA and vinylferrocene
lesson43: TLC Analysis of ferrocene and derivatives
lesson44: Finishing, Clean up
lesson45: Storing laboratory equipment, Clean up

Several reports and tests will be assigned.

The instructors and the contents can be changed depending on the situation.  
Text/Reference
Books,etc.
Lecture style: Organic experiments instructed by teachers
Textbook: Distributed original textbook, and Kagaku Dojin Henshubu eds."Jikken wo anzen ni okonau tameni", Kagaku Dojin
Reference book: Kazuo Hata, Ken-ichi Watanabe, "Kiso jikken kagaku", Maruzen 
PC or AV used in
Class,etc.
 
(More Details) Textbooks and distributed materials 
Learning techniques to be incorporated  
Suggestions on
Preparation and
Review
lesson1-45: Prepare for each experiment. Understand the properties and handrings of the chemical reagents, experimental procedures, and attentions to be paid before starting each experiment. Submit your experiment reports in the designated format by the due date.  
Requirements Prerequisite: "Basic Experiments in Chemistry" 
Grading Method Evaluation will be based on attitude to experiments (40%) and the submitted reports (60%). 60 Points or more at one hundred perfect score will be required for credit. It is necessary to finish all the experiments and to submit all the reports before evaluation. The reports created on PCs will be checked using plagiarism check software, and points may be deducted according to the rate of plagiarism.  
Practical Experience  
Summary of Practical Experience and Class Contents based on it  
Message  
Other   
Please fill in the class improvement questionnaire which is carried out on all classes.
Instructors will reflect on your feedback and utilize the information for improving their teaching. 
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