Academic Year |
2024Year |
School/Graduate School |
School of Engineering |
Lecture Code |
K7113030 |
Subject Classification |
Specialized Education |
Subject Name |
化学実験I |
Subject Name (Katakana) |
カガクジツケン 1 |
Subject Name in English |
Chemical Experiments I |
Instructor |
NAKAYAMA YUUSHOU,KAWASAKI RIKU,ADACHI YOHHEI,MIKIE TSUBASA |
Instructor (Katakana) |
ナカヤマ ユウショウ,カワサキ リク,アダチ ヨウヘイ,ミキエ ツバサ |
Campus |
Higashi-Hiroshima |
Semester/Term |
3rd-Year, First Semester, First Semester |
Days, Periods, and Classrooms |
(1st) Mon5-8,Thur5-8,Fri5-8:ENG B4-008 |
Lesson Style |
Experiment |
Lesson Style (More Details) |
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Chemical Reagents, Glasswares |
Credits |
4.0 |
Class Hours/Week |
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Language of Instruction |
J
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Japanese |
Course Level |
3
:
Undergraduate High-Intermediate
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Course Area(Area) |
25
:
Science and Technology |
Course Area(Discipline) |
07
:
Chemistry |
Eligible Students |
Cluster 3, Applied Chemistry |
Keywords |
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Special Subject for Teacher Education |
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Special Subject |
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Class Status within Educational Program (Applicable only to targeted subjects for undergraduate students) | |
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Criterion referenced Evaluation (Applicable only to targeted subjects for undergraduate students) | Program of Applied Chemistry (Knowledge and Understanding) ・Wide range of basic knowledge on liberal arts and specialized education, and professional basic knowledge on chemistry. ・Advanced technical knowledge of applied chemistry. ・The conception ability based on logical thinking supported by basic and technical knowledge. (Abilities and Skills) ・Creativity to solve various problems related to applied chemistry utilizing acquired knowledge and skills ・Socially acceptable sense of moral and designing ability of research and development, which allow demonstrating the ability to solve issues as a researcher ・engineer. (Comprehensive Abilities) ・Self-motivating and continuous learning ability ・Attitudes actively trying to take multiple approaches for solving problems as an independent researcher or engineer utilizing the following items: information collection, skill improvement, development of research methods, analysis and understanding of research outcomes and results. ・Abilities for logical description, presentation, and discussion in Japanese language. |
Class Objectives /Class Outline |
Students will learn the following contents through the chemical experiments of several organic reactions: ・Building experiment plans ・Handle of the reaction reagents and solvents ・Handle of labwares ・Reaction operations ・Purification of materials (distillation, recrystallization, extraction, reprecipitation, etc.) ・How to write experiment notebook, report ・Various analyses (GC, LC, TLC, IR, NMR, the molecular weight measurement) |
Class Schedule |
lesson1: Guidance lesson2: Theme I Guidance (Installation of ChemDraw, User registration for SciFinder) lesson3: ChemDraw workshop lesson4: SciFinder workshop lesson5: How to write a report lesson6: How to use a rotary evaporator lesson7: Separation of neutral, acidic, and basic compounds lesson8: How to use a chromatography lesson9: Clean up lesson10: How to set up a thin layer chromatography (TLC) analysis lesson11: How to set up a silica-gel chromatography lesson12: Finishing, Clean up lesson13: Theme II Guidance lesson14: Extraction of caffeine from tea lesson15-17: Extraction of pigments from plants and their purification using silicagel column chromatography lesson18: Finishing, Clean up lesson19-20: Preparation of thermo-responsive hydrogel comprising PNIPAM lesson21-22: Synthesis and characterization of methylorange lesson23: Finishing, Clean up lesson24: Theme III Guidance lesson25: Wittig-Horner reaction lesson26: E2 reaction lesson27: Diels-Alder reaction-1 lesson28: Diels-Alder reaction-2 lesson29: Finishing, Clean up lesson30: Aldol reaction lesson31: Cross-coupling reaction lesson32: Synthesis of poly(vinyl acetate) lesson33: Measurement of Molecular Weight lesson34: Finishing, Clean up lesson35: Theme IV guidance lesson36-37: Synthesis of ferrocene lesson38: Synthesis of acetylferrocene lesson39: TLC Analysis of acetylferrocene, Synthesis of 1-hydroxyethylferrocene lesson40: Synthesis of vinylferrocene lesson41-42: Copolymerization of MMA and vinylferrocene lesson43: TLC Analysis of ferrocene and derivatives lesson44: Finishing, Clean up lesson45: Storing laboratory equipment, Clean up
Several reports and tests will be assigned.
The instructors and the contents can be changed depending on the situation. |
Text/Reference Books,etc. |
Lecture style: Organic experiments instructed by teachers Textbook: Distributed original textbook, and Kagaku Dojin Henshubu eds."Jikken wo anzen ni okonau tameni", Kagaku Dojin Reference book: Kazuo Hata, Ken-ichi Watanabe, "Kiso jikken kagaku", Maruzen |
PC or AV used in Class,etc. |
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(More Details) |
Textbooks and distributed materials |
Learning techniques to be incorporated |
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Suggestions on Preparation and Review |
lesson1-45: Prepare for each experiment. Understand the properties and handrings of the chemical reagents, experimental procedures, and attentions to be paid before starting each experiment. Submit your experiment reports in the designated format by the due date. |
Requirements |
Prerequisite: "Basic Experiments in Chemistry" |
Grading Method |
Evaluation will be based on attitude to experiments (40%) and the submitted reports (60%). 60 Points or more at one hundred perfect score will be required for credit. It is necessary to finish all the experiments and to submit all the reports before evaluation. The reports created on PCs will be checked using plagiarism check software, and points may be deducted according to the rate of plagiarism. |
Practical Experience |
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Summary of Practical Experience and Class Contents based on it |
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Message |
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Other |
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Please fill in the class improvement questionnaire which is carried out on all classes. Instructors will reflect on your feedback and utilize the information for improving their teaching. |