Hiroshima University Syllabus

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Japanese
Academic Year 2020Year School/Graduate School School of Engineering
Lecture Code K7113030 Subject Classification Specialized Education
Subject Name 化学実験I
Subject Name
(Katakana)
カガクジツケン 1
Subject Name in
English
Chemical Experiments I
Instructor NAKAYAMA YUUSHIYOU,KAWASAKI RIKU,KOMEYAMA KIMIHIRO,TANAKA RYO,SUGIKAWA KOTA,ADACHI YOHHEI
Instructor
(Katakana)
ナカヤマ ユウショウ,カワサキ リク,コメヤマ キミヒロ,タナカ リョウ,スギカワ コウタ,アダチ ヨウヘイ
Campus Higashi-Hiroshima Semester/Term 3rd-Year,  First Semester,  First Semester
Days, Periods, and Classrooms (1st) Mon5-8,Thur5-8,Fri5-8
Lesson Style Experiment Lesson Style
【More Details】
Chemical Reagents, Glasswares 
Credits 4 Class Hours/Week   Language on Instruction J : Japanese
Course Level 3 : Undergraduate High-Intermediate
Course Area(Area) 25 : Science and Technology
Course Area(Discipline) 07 : Chemistry
Eligible Students Cluster 3, Applied Chemistry
Keywords  
Special Subject for Teacher Education   Special Subject  
Class Status
within Educational
Program
 
Criterion referenced
Evaluation
Program of Applied Chemistry
(Knowledge and Understanding)
・Wide range of basic knowledge on liberal arts and specialized education, and professional basic knowledge on chemistry.
・Advanced technical knowledge of applied chemistry.
・The conception ability based on logical thinking supported by basic and technical knowledge.
(Abilities and Skills)
・Creativity to solve various problems related to applied chemistry utilizing acquired knowledge and skills
・Socially acceptable sense of moral and designing ability of research and development, which allow demonstrating the ability to solve issues as a researcher ・engineer.
(Comprehensive Abilities)
・Self-motivating and continuous learning ability
・Attitudes actively trying to take multiple approaches for solving problems as an independent researcher or engineer utilizing the following items: information collection, skill improvement, development of research methods, analysis and understanding of research outcomes and results.
・Abilities for logical description, presentation, and discussion in Japanese language. 
Class Objectives
/Class Outline
Students will learn the following contents through the chemical experiments of several organic reactions:
・Building experiment plans
・Handle of the reaction reagents and solvents
・Handle of labwares
・Reaction operations
・Purification of materials (distillation, recrystallization, extraction, reprecipitation, etc.)
・How to write experiment notebook, report
・Various analyses (GC, LC, TLC, IR, NMR, the molecular weight measurement)
・Glassworks 
Class Schedule lesson1-3: Training courses for SciFinder
lesson4-7: Training courses for ChemDraw
lesson8: Guidance
lesson9-10: Synthesis of iodobenzene by diazotization of aniline
lesson11: Synthesis of p-iodoaniline
lesson12: Melting point measurement, Analysis of spectra
lesson13: Synthesis of Nylon-6,6 by Interfacial Polymerization
lesson14-16: Synthesis of Poly(vinyl acetate) (Radical Polymerization), Measurement of its Molecular Weight
lesson17-18: Extraction and purification of pigments from plant leaves by silica gel column chromatography
lesson19-20: Synthesis of isoamyl acetate
lesson21: Synthesis of temperature-responsive polymers and gels
lesson22-23: Synthesis of temperature-responsive dyes (Diazotization and coupling)
lesson24: Evaluation of temperature-responsive materials
lesson25: Guidance, Synthesis of acetylferrocene
lesson26: TLC Analysis of acetylferrocene, Synthesis of 1-hydroxyethylferrocene
lesson27: Synthesis of vinylferrocene
lesson28: Copolymerization of MMA and vinylferrocene
lesson29: TLC Analysis of ferrocene and derivatives
lesson30: Finishing
The schedule could be changed depending on the situation of COVID-19.

Several reports and tests will be assigned.  
Text/Reference
Books,etc.
Lecture style: Organic experiments instructed by teachers
Textbook: Distributed original textbook, and "Jikken wo anzen ni okonau tameni", Kagaku Dojin
Reference book: Kazuo Hata, Ken-ichi Watanabe, "Kiso jikken kagaku", Maruzen 
PC or AV used in
Class,etc.
Textbooks and distributed materials 
Suggestions on
Preparation and
Review
lesson1-30: Prepare for each experiment. Understand the properties and handrings of the chemical reagents, experimental procedures, and attentions to be paid before starting each experiment. Submit the experiment reports according to a designated form by time limit.  
Requirements Prerequisite: "Basic Experiments in Chemistry" 
Grading Method Evaluation will be based on attitude to experiments (40%) and the submitted reports (60%). 60 Points or more at one hundred perfect score will be required for credit. It is necessary to finish all the experiments and to submit all the reports before evaluation.  
Practical Experience  
Summary of Practical Experience and Class Contents based on it  
Message  
Other   
Please fill in the class improvement questionnaire which is carried out on all classes.
Instructors will reflect on your feedback and utilize the information for improving their teaching. 
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